Isopropylacetoacetate与CAS542-08-5

CAS:542-08-5
Molecular Formula:C7H12O3
Molecular Weight:144.17
EINECS:208-798-4

Synonyms:3-oxo-butanoicaci1-methylethylester; 3-Oxobutansαure-1-methylethylester;3-Oxo-butyricacidisopropylester; Acetoaceticacid,isopropylester; acetoaceticacidisopropylester; Butanoicacid,3-oxo-,1-methylethylester; 3-oxobutanoic acid propan-2-yl ester; Isopropyl3-oxobutanoate; Isopropyl3-oxobutyrate

Isopropylacetoacetate与CAS542-08-5
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什么是的Isopropylacetoacetate与CAS542-08-5?

In a 500ml flask equipped with a stirrer, thermometer, and reflux condenser, 150g (2.5mol) of isopropanol and 0.36g of triethylamine were added. 210g (2.5mol) of diethylene ketone was added dropwise at room temperature. The reaction temperature was controlled at 70 ℃ during the process, and the dropwise addition was completed. The temperature was kept at 70 ℃ for 6 hours to complete the reaction. The crude ester was subjected to negative pressure distillation to obtain the final product Isopropyl acetoacetate 343g, with a yield of 95.2% and a content of 99.3%.

规格

项目

结果,

外观

液体

含量

99.0%min

湿气

<0.04%

重金属

<0.002%

沸点

95°C52hPa

熔点

-27°C

折射率

n20/D1.418

应用

乙酰乙酸异丙酯用于作为中间体用于制造农用化学品和药品,如伊拉地平。

包装

通常装在25公斤/桶,并且还可以做的定制软件包。

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Isopropylacetoacetate与CAS542-08-5
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